1H谱最新氘代试1
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责编:小OO
时间:2025-09-28 12:30:40
1H谱最新氘代试1
1H谱最新氘代试剂(核磁试剂)化学位移表碳原子氘代四氢呋喃氘代二氯甲烷氘代氯仿氘代甲苯氘代苯氘代氯苯氘代丙酮氘代DMSO氘代乙腈氘代三氟乙醇氘代甲醇氘代水氘代试剂位移1.725.327.262.087.166.962.052.501.945.023.314.79 3.58 6.97 6.99 3.88 7.01 7.14 7.09 水峰OHs2.461.521.560.430.401.032.84b3.33b2.133.6.87
导读1H谱最新氘代试剂(核磁试剂)化学位移表碳原子氘代四氢呋喃氘代二氯甲烷氘代氯仿氘代甲苯氘代苯氘代氯苯氘代丙酮氘代DMSO氘代乙腈氘代三氟乙醇氘代甲醇氘代水氘代试剂位移1.725.327.262.087.166.962.052.501.945.023.314.79 3.58 6.97 6.99 3.88 7.01 7.14 7.09 水峰OHs2.461.521.560.430.401.032.84b3.33b2.133.6.87
1H谱最新氘代试剂(核磁试剂)化学位移表 |
碳原子 | 氘代四氢呋喃 | 氘代二氯甲烷 | 氘代氯仿 | 氘代甲苯 | 氘代苯 | 氘代氯苯 | 氘代丙酮 | 氘代DMSO | 氘代乙腈 | 氘代三氟乙醇 | 氘代甲醇 | 氘代水 |
氘代试剂位移 | 1.72 | 5.32 | 7.26 | 2.08 | 7.16 | 6.96 | 2.05 | 2.50 | 1.94 | 5.02 | 3.31 | 4.79 |
| | | 3.58 | | | 6.97 | | 6.99 | | | | 3.88 | | |
| | | | | | 7.01 | | 7.14 | | | | | | |
| | | | | | 7.09 | | | | | | | | |
水峰 | OH | s | 2.46 | 1.52 | 1.56 | 0.43 | 0.40 | 1.03 | 2.84b | 3.33b | 2.13 | 3.66 | 4.87 | |
乙酸 | acetic | acid | CH3 | s | 1. | 2.06 | 2.10 | 1.57 | 1.52 | 1.76 | 1.96 | 1.91 | 1.96 | 2.06 |
丙酮 | CH3 | s | 2.05 | 2.12 | 2.17 | 1.57 | 1.55 | 1.77 | 2.09 | 2.09 | 2.08 | 2.19 | 2.15 | 2.22 |
乙腈 | CH3 | s | 1.95 | 1.97 | 2.10 | 0.69 | 0.58 | 1.21 | 2.05 | 2.07 | 1.96 | 1.95 | 2.03 | 2.06 |
苯 | CH | s | 7.31 | 7.35 | 7.36 | 7.12 | 7.15 | 7.20 | 7.36 | 7.37 | 7.37 | 7.36 | 7.33 | |
正丁醇 | CH3 | s | 1.15 | 1.24 | 1.28 | 1.03 | 1.05 | 1.12 | 1.18 | 1.11 | 1.16 | 1.28 | 1.40 | 1.24 |
| OH | sc | 3.16 | | | | 0.58 | 0.63 | 1.30 | 4.19 | 2.18 | 2.20 | | |
氯仿 | CH | s | 7. | 7.32 | 7.26 | 6.10 | 6.15 | 6.74 | 8.02 | 8.32 | 7.58 | 7.33 | 7.90 | |
18-冠醚-6 | CH2 | s | 3.57 | 3.59 | 3.67 | 3.36 | 3.39 | 3.41 | 3.59 | 3.51 | 3.51 | 3. | 3. | 3.80 |
DMF | CH | s | 7.91 | 7.96 | 8.02 | 7.57 | 7.63 | 7.73 | 7.96 | 7.95 | 7.92 | 7.86 | 7.97 | 7.92 |
| CH3 | s | 2.88 | 2.91 | 2.96 | 2.37 | 2.36 | 2.51 | 2.94 | 2. | 2. | 2.98 | 2.99 | 3.01 |
| CH3 | s | 2.76 | 2.82 | 2.88 | 1.96 | 1.86 | 2.30 | 2.78 | 2.73 | 2.77 | 2.88 | 2.86 | 2.85 |
二恶烷 | CH2 | s | 3.56 | 3.65 | 3.71 | 3.33 | 3.35 | 3.45 | 3.59 | 3.57 | 3.60 | 3.76 | 3.66 | 3.75 |
DME | CH3 | s | 3.28 | 3.34 | 3.40 | 3.12 | 3.12 | 3.17 | 3.28 | 3.24 | 3.28 | 3.40 | 3.35 | 3.37 |
| CH2 | s | 3.43 | 3.49 | 3.55 | 3.31 | 3.33 | 3.37 | 3.46 | 3.43 | 3.45 | 3.61 | 3.52 | 3.60 |
乙烷 | CH3 | s | 0.85 | 0.85 | 0.87 | 0.81 | 0.80 | 0.79 | 0.83 | 0.82 | 0.85 | 0.85 | 0.85 | 0.82 |
乙醇 | CH3 | t, 7 | 1.10 | 1.19 | 1.25 | 0.97 | 0.96 | 1.06 | 1.12 | 1.06 | 1.12 | 1.22 | 1.19 | 1.17 |
| CH2 | q, 7d | 3.51 | 3.66 | 3.72 | 3.36 | 3.34 | 3.51 | 3.57 | 3.44 | 3.54 | 3.71 | 3.60 | 3.65 |
| OH | sc, | 3.30 | 1.33 | 1.32 | 0.83 | 0.50 | 1.39 | 3.39 | 4.63 | 2.47 | 59.68 | 58.26 | 58.05 |
环己胺 | CH2 | s | 1.44 | 1.44 | 1.43 | 1.40 | 1.40 | 1.37 | 1.43 | 1.40 | 1.44 | 1.47 | 1.45 | |
二氯乙烷 | CH2 | s | 3.77 | 3.76 | 3.73 | 2.91 | 2.90 | 3.26 | 3.87 | 3.90 | 3.81 | 3.71 | 3.78 | |
二氯甲烷 | CH2 | s | 5.51 | 5.33 | 5.30 | 4.32 | 4.27 | 4.77 | 5.63 | 5.76 | 5.44 | 5.24 | 5.49 | |
乙醚 | CH3 | t, 7 | 1.12 | 1.15 | 1.21 | 1.10 | 1.11 | 1.10 | 1.11 | 1.09 | 1.12 | 1.20 | 1.18 | 1.17 |
| CH2 | q, 7 | 3.38 | 3.43 | 3.48 | 3.25 | 3.26 | 3.31 | 3.41 | 3.38 | 3.42 | 3.58 | 3.49 | 3.56 |
二甘醇二甲醚 | CH2 | m | 3.43 | 3.57 | 3.65 | 3.43 | 3.46 | 3.49 | 3.56 | 3.51 | 3.53 | 3.67 | 3.61 | 3.67 |
| CH2 | m | 3.53 | 3.50 | 3.57 | 3.31 | 3.34 | 3.37 | 3.47 | 3.38 | 3.45 | 3.62 | 3.58 | 3.61 |
| OCH3 | s | 3.28 | 3.33 | 3.39 | 3.12 | 3.11 | 3.16 | 3.28 | 3.24 | 3.29 | 3.41 | 3.35 | 3.37 |
乙酸乙酯 | CH3CO | s | 1.94 | 2.00 | 2.05 | 1.69 | 1.65 | 1.78 | 1.97 | 1.99 | 1.97 | 2.03 | 2.01 | 2.07 |
| CH2 | q, 7 | 4.04 | 4.08 | 4.12 | 3.87 | 3. | 3.96 | 4.05 | 4.03 | 4.06 | 4.14 | 4.09 | 4.14 |
| CH3 | t, 7 | 1.19 | 1.23 | 1.26 | 0.94 | 0.92 | 1.04 | 1.20 | 1.17 | 1.20 | 1.26 | 1.24 | 1.24 |
乙烯 | CH2 | s | 5.36 | 5.40 | 5.40 | 5.25 | 5.25 | 5.29 | 5.38 | 5.41 | 5.41 | 5.40 | 5.39 | 5.44 |
乙二醇 | CH2 | se | 3.48 | 3.66 | 3.76 | 3.36 | 3.41 | 3.58 | 3.28 | 3.34 | 3.51 | 3.72 | 3.59 | 3.65 |
六甲基苯 | CH3 | s | 2.18 | 2.20 | 2.24 | 2.10 | 2.13 | 2.10 | 2.17 | 2.14 | 2.19 | 2.24 | 2.19 | |
正己烷 | CH3 | t, 7 | 0. | 0. | 0.88 | 0.88 | 0. | 0.85 | 0.88 | 0.86 | 0. | 0.91 | 0.90 | |
| CH2 | m | 1.29 | 1.27 | 1.26 | 1.22 | 1.24 | 1.19 | 1.28 | 1.25 | 1.28 | 1.31 | 1.29 | |
吡啶 | CH(2,6) | m | 8.54 | 8.59 | 8.62 | 8.47 | 8.53 | 8.51 | 8.58 | 8.58 | 8.57 | 8.45 | 8.53 | 8.52 |
| CH(3,5) | m | 7.25 | 7.28 | 7.29 | 6.67 | 6.66 | 6.90 | 7.35 | 7.39 | 7.33 | 7.40 | 7.44 | 7.45 |
| CH(4) | m | 7.65 | 7.68 | 7.68 | 6.99 | 6.98 | 7.25 | 7.76 | 7.79 | 7.73 | 7.82 | 7.85 | 7.87 |
吡咯 | NH | br | t | 9.96 | 8.69 | 8.40 | 7.71 | 7.80 | 8.61 | 10.02 | 10.75 | 119.61 | 118.28 | 119.06 |
| CH(2,5) | m | 6.66 | 6.79 | 6.83 | 6.43 | 6.48 | 6.62 | 6.77 | 6.73 | 6.75 | 6.84 | 6.72 | 6.93 |
| CH(3,4) | m | 6.02 | 6.19 | 6.26 | 6.27 | 6.37 | 6.27 | 6.07 | 6.01 | 6.10 | 6.24 | 6.08 | 6.26 |
吡咯啉 | CH2(2,5) | m | 2.75 | 2.82 | 2.87 | 2.54 | 2.54 | 2. | | 2.67 | 2.75 | 3.11 | 2.80 | 3.07 |
| CH2(3,4) | m | 1.59 | 1.67 | 1.68 | 1.36 | 1.33 | 1.43 | | 1.55 | 1.61 | 1.93 | 1.72 | 1.87 |
硅脂 | CH3 | s | 0.11 | 0.09 | 0.07 | 0.26 | 0.29 | 0.14 | 0.13 | -0.06 | 0.08 | 0.16 | 0.10 | |
四氢呋喃 | CH2(2,5) | m | 3.62 | 3.69 | 3.76 | 3.54 | 3.57 | 3.59 | 3.63 | 3.60 | 3. | 3.78 | 3.71 | 3.74 |
| CH2(3,4) | m | 1.79 | 1.82 | 1.85 | 1.43 | 1.40 | 1.55 | 1.79 | 1.76 | 1.80 | 1.91 | 1.87 | 1.88 |
甲苯 | CH3 | s | 2.31 | 2.34 | 2.36 | 2.11 | 2.11 | 2.16 | 2.32 | 2.30 | 2.33 | 2.33 | 2.32 | |
| CH(2,4,6) | m | 7.10 | 7.15 | 7.17 | 6.96-7.01 | 7.02 | 7.01-7.08 | 7.10-7.20 | 7.18 | 7.10-7.30 | 7.10-7.30 | 7.16 | |
| CH(3,5) | m | 7.19 | 7.24 | 7.25 | 7.09 | 7.13 | 7.10-7.17 | 7.10-7.20 | 7.18 | 7.10-7.30 | 7.10-7.30 | 7.16 | |
三乙胺 | CH3 | t | 0.97 | 0.99 | 1.03 | 0.95 | 0.96 | 0.93 | 0.96 | 0.93 | 0.96 | 1.31 | 1.05 | 0.99 |
| CH2 | q | 2.46 | 2.48 | 2.53 | 2.39 | 2.40 | 2.39 | 2.45 | 2.43a | 2.45 | 3.12 | 2.58 | 2.57 |
六甲基二硅醚 | CH3 | s | 0.07 | 0.07 | 0.07 | 0.10 | 0.12 | 0.10 | 0.07 | 0.06 | 0.07 | 0.08 | 0.07 | 0.28 |
HMPAc | CH3 | d | 2.58 | 2.60 | 2.65 | 2.42 | 2.40 | 2.47 | 2.59 | 2.53 | 2.57 | 2.63 | 2. | 2.61 |
咪唑 | H2 | s | 4.55 | 4.59 | 4.62 | 4.50 | 4.47 | 4.49 | 4.54 | 4.61 | 4.57 | 4.53 | 4.56 | H2 |
甲烷 | CH4 | s | 0.19 | 0.21 | 0.22 | 0.17 | 0.16 | 0.15 | 0.17 | 0.20 | 0.20 | 0.18 | 0.20 | |
甲醇 | CH3 | s | 3.27 | 3.42 | 3.49 | 3.03 | 3.07 | 3.25 | 3.31 | 3.16 | 3.28 | 3.44 | 3.34 | 3.34 |
| OH | S | 3.02 | 1.09 | 1.09 | | | 1.30 | 3.12 | 4.01 | 2.16 | | | |
硝基甲烷 | CH3 | s | 4.31 | 4.31 | 4.33 | 3.01 | 2.94 | 3.59 | 4.43 | 4.42 | 4.31 | 4.28 | 4.34 | 4.40 |
正戊烷 | CH3 | t | 0. | 0. | 0.88 | 0.87 | 0.87 | 0.84 | 0.88 | 0.86 | 0. | 0.90 | 0.90 | |
| CH2 | m | 1.31 | 1.30 | 1.27 | 1.25 | 1.23 | 1.23 | 1.27 | 1.27 | 1.29 | 1.33 | 1.29 | |
丙烷 | CH3 | t | 0.90 | 0.90 | 0.90 | 0. | 0.86 | 0.84 | 0.88 | 0.87 | 0.90 | 0.90 | 0.91 | 0.88 |
| CH2 | sept | 1.33 | 1.32 | 1.32 | 1.32 | 1.26 | 1.26 | 1.31 | 1.29 | 1.33 | 1.33 | 1.34 | 1.30 |
2-丙醇 | CH3 | d | 1.08 | 1.17 | 1.22 | 0.95 | 0.95 | 1.04 | 1.10 | 1.04 | 1.09 | 1.20 | 1.50 | 1.17 |
| CH | sept | 3.82 | 3.97 | 4.04 | 3.65 | 3.67 | 3.82 | 3.90 | 3.78 | 3.87 | 4.05 | 3.92 | 4.02 |
丙烯 | CH3 | dt | 1.69 | 1.71 | 1.73 | 1.55 | 1.55 | 1.58 | 1.68 | 1.68 | 1.70 | 1.70 | 1.70 | 1.70 |
| CH2(1) | dm | 4. | 4.93 | 4.94 | 4.92 | 4.95 | 4.91 | 4.90 | 4.94 | 4.93 | 4.93 | 4.91 | 4.95 |
| CH2(2) | dm | 4.99 | 5.03 | 5.03 | 4.98 | 5.01 | 4.98 | 5.00 | 5.03 | 5.04 | 5.03 | 5.01 | 5.06 |
| CH | m | 5.79 | 5.84 | 5.83 | 5.70 | 5.72 | 5.72 | 5.81 | 5.80 | 5.85 | 5.87 | 5.82 | 5.90 |
吡啶 | CH(2,6) | m | 8.54 | 8.59 | 8.62 | 8.47 | 8.53 | 8.51 | 8.58 | 8.58 | 8.57 | 8.45 | 8.53 | 8.52 |
| CH(3,5) | m | 7.25 | 7.28 | 7.29 | 6.67 | 6.66 | 6.90 | 7.35 | 7.39 | 7.33 | 7.40 | 7.44 | 7.45 |
| CH(4) | m | 7.65 | 7.68 | 7.68 | 6.99 | 6.98 | 7.25 | 7.76 | 7.79 | 7.73 | 7.82 | 7.85 | 7.87 |
1H谱最新氘代试1
1H谱最新氘代试剂(核磁试剂)化学位移表碳原子氘代四氢呋喃氘代二氯甲烷氘代氯仿氘代甲苯氘代苯氘代氯苯氘代丙酮氘代DMSO氘代乙腈氘代三氟乙醇氘代甲醇氘代水氘代试剂位移1.725.327.262.087.166.962.052.501.945.023.314.79 3.58 6.97 6.99 3.88 7.01 7.14 7.09 水峰OHs2.461.521.560.430.401.032.84b3.33b2.133.6.87